Sintered Si3N4 for High Performance Thermomechanical Applications

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Abstract:

The gas pressure sintering GPS process for dense 99 Si3N4 containing approx. 7 wt BeSiN2 and 7 wt SiO2 as sintering aids was scaled-up to develop a property data base for use in thermomechanical applications at high approx. 1300 deg C temperatures. The fracture strength in 3-pt bend for test bars approx. 0.6 cm x 0.6 cm x 4.5 cm long was approx. 440 MNm-2 63,700 psi for a span length of 3.8 cm. There was little drop 15 in high temperature strength at 1400 deg C in air. The creep resistance was outstanding at 1300 to 1400 deg C, as evidenced by creep rates of approx. 4 x .00001h for a stress of 207 MPa 30,000 psi at 1400 C.

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