Synthesis of -1-Sila-2-Azacyclopentane Ring Compounds

reportActive / Technical Report | Accession Number: AD0714552 | Open PDF

Abstract:

New ring-compounds 1,1-diethoxy-2-triphenylsilyl-1-sila-2- azacyclopentane, 1,1-diethoxy-2-ethoxydimethylsilyl-1-sila-2-azacyclopentane, and tri-1-ethoxy-1-sila-2-azacyclopentane were prepared and isolated. The third compound reacts with ethyl alcohol to form 3-aminopropyltriethoxysilane and with phenyllithium and ethyllithium to form tri-1-phenyl-1-sila-2- azacyclopentane and tri-1-ethyl1-sila-2-azacyclopentane, respectively.

Author(s):
Tsai, Tsu-tzu
Author Organization(s):
AIR FORCE MATERIALS LAB WRIGHT-PATTERSON AFB OH
Descriptive Note:
Technical rept. Nov 1968-Mar 1970
Supplementary Note:
DOI: 10.21236/AD0714552
Pagination:
0026

Security Markings

DOCUMENT & CONTEXTUAL SUMMARY

Distribution:
Approved For Public Release, Document Partially Illegible
Distribution Statement:
Availability: Document Partially Illegible.

RECORD

Collection: TR
Identifying Numbers
Report Number(s):
AFML-TR-70-116
Task Number(s):
734201
Project Number(s):
AF-7342
Monitor Series:
AFML
 Subject Terms
Joint Capability Areas:
JCA_5_Command and Control; JCA_6.3.3_Spectrum Management; JCA_5.3_Planning; JCA_6.3_Net Management; JCA_6_Net Centric; JCA_1.3_Human Capital Management; JCA_1_Force Support; JCA_1.3.2_Personnel Management
Communities of Interest:
C4I
Descriptor(s):
*SILANES, *INFRARED SPECTRA, SYNTHESIS(CHEMISTRY), SILOXANES, AMINES, AMMONIUM COMPOUNDS, LITHIUM COMPOUNDS
Field(s)/Group(s):
Organic Chemistry
Keyword(s):
*PROPYLAMINE TRIETHOXYSILYL, *SILICON HETEROCYCLIC COMPOUNDS
Report Date:
1970 Sep 01