X-RAY POWDER PATTERNS FOR THE IDENTIFICATION OF SOME N-ALKANONE SEMICARBAZONES.

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Abstract:

The interplanar spacings obtained from the X-ray powder patterns of a series of structurally related semicarbazones were used to unequivocally identify the ketones from which the derivatives were prepared. The advantages of the proposed over the currently used melting points to identify the compounds were cited. The method was found to be applicable to slightly contaminated mixtures of semicarbazones. Author

Author(s):
Radell, Jack ; Brodman, Bruce W. ; Kramer, Kimball
Author Organization(s):
FRANKFORD ARSENAL PHILADELPHIA PA PITMAN-DUNN RESEARCH LABS
Descriptive Note:
Technical research article,
Supplementary Note:
Pub. in Canadian Journal of Chemistry v43 p1661-4 1965 (Copies available only to DDC users).
Annotation:
Reprint: X-ray powder patterns for the identification of some n-alkanone semicarbazones.
Pagination:
0007

Security Markings

DOCUMENT & CONTEXTUAL SUMMARY

Distribution:
Approved For Public Release

RECORD

Collection: TR
Identifying Numbers
Report Number(s):
A65-5
Project Number(s):
1CO14501B13A
 Subject Terms
Communities of Interest:
No COI(s) Identified
Descriptor(s):
(*KETONES, X RAY DIFFRACTION), (*HYDRAZINE DERIVATIVES, X RAY DIFFRACTION), (*X RAY DIFFRACTION, KETONES), CHEMICAL BONDS, IMPURITIES
Keyword(s):
SEMICARBAZONES
Report Date:
1964 Dec 16