PREPARATION OF HIGH PURITY ANHYDROUS FERROUS CHLORIDE

reportActive / Technical Report | Accession Number: AD0403265 | Open PDF

Abstract:

Several methods for preparing high purity anhydrous ferrous chloride were investigated. The technique finally developed involved the high temperature chlorination of iron sponge with anhydrous hydrogen chloride and collection of the sublimed ferrous chloride in a condenser held at such a temperature that ferric chloride did not condense. Ferric iron was undetectable in the final product and other impurities were well below the specified limits. Over 3 kilograms of high purity anhydrous ferrous chloride were pre pared by this technique.

Author(s):
Chandler, Horace W. ; Malgiolio, Joseph
Author Organization(s):
ISOMET CORP OAKLAND NJ
Descriptive Note:
Summary rept., 14 Mar 1961-14 Sep 1962
Supplementary Note:
DOI: 10.21236/AD0403265
Pagination:
0023

Security Markings

DOCUMENT & CONTEXTUAL SUMMARY

Distribution:
Approved For Public Release
Distribution Statement:
Approved For Public Release; Distribution Is Unlimited.

RECORD

Collection: TR
Identifying Numbers
Report Number(s):
ASD-TDR-62-1040
Contract/Grant Number(s):
AF 33(616)-8187
Task Number(s):
73530
Project Number(s):
7353
Monitor Series:
TDR-62-1040, ASD
 Subject Terms
Joint Capability Areas:
JCA_5_Command and Control; JCA_5.3_Planning; JCA_6_Net Centric; JCA_6.4.1_Secure Information Exchange; JCA_3.2_Engagement; JCA_3_Force Application
Modernization Areas:
Microelectronics
Communities of Interest:
Weapons Technologies
Descriptor(s):
*SYNTHESIS(CHEMISTRY), *IRON COMPOUNDS, *CHLORIDES, SPECTROSCOPY, NICKEL, IRON, ENERGY
Field(s)/Group(s):
Physical Chemistry
Keyword(s):
*FERROUS CHLORIDE, ANHYDROUS FERROUS CHLORIDE
Report Date:
1963 Mar 01