Accession Number:

ADD015530

Title:

Synthesis of Aminonitrobenzodifuroxan.

Descriptive Note:

Patent, Filed 1 Oct 90, patented 22 Sep 92,

Corporate Author:

DEPARTMENT OF THE NAVY WASHINGTON DC

Report Date:

1992-09-22

Pagination or Media Count:

9.0

Abstract:

Aminonitrobenzodifuroxan CL-18 is prepared by directly converting pentanitroaniline to aminonitrobenzodifuroxan with heat in the presence of an excess of sodium azide. The pentanitroaniline is prepared in high yield from 3,5-dinitroaniline with a mixture of nitric acid and sulfuric acid in which the final sulfuric acid concentration is from 99.0 to 99.5.

Subject Categories:

  • Organic Chemistry
  • Ammunition and Explosives
  • Physical Chemistry

Distribution Statement:

APPROVED FOR PUBLIC RELEASE