Accession Number:
ADA581116
Title:
3,3'-(1-Oxopropane-1,3-diyl)bis(1,3-thiazolidine-2-thione) Chlorobenzene Hemisolvate
Descriptive Note:
Journal article
Corporate Author:
NAVAL RESEARCH LAB WASHINGTON DC CHEMISTRY DIV
Personal Author(s):
Report Date:
2013-01-01
Pagination or Media Count:
9.0
Abstract:
The title compound, C9H12N2OS40.5C6H5Cl, which contains two 1,3-thiazolidine-2-thione rings, is a by-product of the synthesis of 3-acryloyl-1,3-thiazolidine-2-thione. The dihedral angle between these rings is 79.95 9 deg., with both rings displaying a twisted conformation. The twist angle of the amide group is 5.6 1 deg. In the crystal, the molecules are linked into 001 chains by C--H...O interactions. The chlorobenzene solvent molecule was found to show unresolvable disorder about a centre of inversion and its contribution to the scattering was removed with the SQUEEZE option in PLATON Spek 2009. Acta Cryst. D65, 148 155.
Descriptors:
Subject Categories:
- Organic Chemistry