Accession Number:

ADA089044

Title:

A Diglyme Adduct of Tin(IV) Chloride Formed on Drying Aromatic Solvents by the Benzophenone Ketyl/Potassium Metal Method,

Descriptive Note:

Corporate Author:

OKLAHOMA UNIV NORMAN DEPT OF CHEMISTRY

Personal Author(s):

Report Date:

1980-08-15

Pagination or Media Count:

7.0

Abstract:

Use of diglyme diethyleneglycoldimethylether for solubilization in the benzophenone ketylpotassium metal method for drying and deoxygenating aromatic solvents can result in contamination of the distilled solvent with subsequent formation of adducts with Lewis acids. The diglyme adduct of tinIV chloride is isolated, and the magnitude of its tin-119m Mossbauer Quadrupole Splitting interpreted in terms of its structure. Author

Subject Categories:

  • Inorganic Chemistry
  • Organic Chemistry

Distribution Statement:

APPROVED FOR PUBLIC RELEASE