Accession Number:

AD0893148

Title:

Chemistry of Catenated Nitrogen Compounds.

Descriptive Note:

Final rept. 11 Apr 71-11 Apr 72,

Corporate Author:

ROCKETDYNE CANOGA PARK CA

Personal Author(s):

Report Date:

1972-04-01

Pagination or Media Count:

28.0

Abstract:

Studies were conducted on the preparation and characterization of triazanium salts. A method was devised for synthesis of 2,2-dimethyltriazanium sulfate. The sulfate was converted to its perchlorate and nitrate by metathetical reactions. The isomer 1,1-dimethyltriazanium bisulfate was also prepared, but its conversion to the perchlorate was not successful. Triazanium bisulfate and methylsulfonate were prepared and characterized by ir spectroscopy. A hydrated triazanium perchlorate was apparently prepared, but attempts to obtain the anhydrous salt gave only decomposition products. Author

Subject Categories:

  • Inorganic Chemistry
  • Organic Chemistry

Distribution Statement:

APPROVED FOR PUBLIC RELEASE