Chemistry of Catenated Nitrogen Compounds.
Final rept. 11 Apr 71-11 Apr 72,
ROCKETDYNE CANOGA PARK CA
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Studies were conducted on the preparation and characterization of triazanium salts. A method was devised for synthesis of 2,2-dimethyltriazanium sulfate. The sulfate was converted to its perchlorate and nitrate by metathetical reactions. The isomer 1,1-dimethyltriazanium bisulfate was also prepared, but its conversion to the perchlorate was not successful. Triazanium bisulfate and methylsulfonate were prepared and characterized by ir spectroscopy. A hydrated triazanium perchlorate was apparently prepared, but attempts to obtain the anhydrous salt gave only decomposition products. Author
- Inorganic Chemistry
- Organic Chemistry