SYNTHESIS AND STUDY OF MONO-O-PHENANTHROLINE CHROMIUM (III) PERCHLORATE.
Technical rept. Jul-Dec 66,
AIR FORCE MATERIALS LAB WRIGHT-PATTERSON AFB OH
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The mono-o-phenanthroline chromium III perchlorate complex is prepared by two separate methods, 1 direct addition of the base to the metal ion in acid solution and heating, and 2 the use of CrII to catalyze the reaction. The desired complex is then isolated by ion-exchange methods, and determined by spectrophotometric and elemental microanalytical procedures. Polarographic information is also given. Author
- Organic Chemistry