Preparation of Derivatives of Iminoborane.
Final rept. 1 Mar 70-30 Jun 73,
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An investigation into synthesis and isolability of derivatives of iminoborane, HBNH, is reported. The pyrolytic method first described has been shown to be less effective than initially believed. A chemical synthesis from arylboron dichloride and primary amines is described. The state of characterization of compounds ArBNR where ArC6F5 and RC6H4OCH3, C6H2CH33, i-C3H7, and i-C4H9 is discussed. Additional experiments necessary for complete confidence in structural assignment are described. Some preliminary results concerning the free radical reactions of P2F4 are also described. Author
- Organic Chemistry