Gas-Liquid Chromatographic Assay of 1,2,3-Trimercaptopropane in Dimercaprol.
Technical rept. Apr 68-Mar 72,
EDGEWOOD ARSENAL MD
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The report provides a description of studies conducted, using the technique of gas-liquid chromatography, to determine if 1,2,3-Trimercaptopropane TSH is present to an extent greater than 1.5 percent in lots of dimercaprol BAL, which is used in the formulation of FSN 6505-108-8500 Dimercaprol Injection, USP, 10 percent 5 cc. Satisfactory results were obtained using an 18-foot glass column, SE-30 liquid support, and isothermal operation. Author
- Organic Chemistry