Accession Number:

AD0753398

Title:

Synthesis of (2-Cyanoethyl)-Amides for Applications in Gas Chromatography

Descriptive Note:

Final rept.

Corporate Author:

SOUTHWEST RESEARCH INST SAN ANTONIO TX BELVOIR FUELS AND LUBRICANTS RESEARCH FACILITY

Personal Author(s):

• Fodor, George E.

Report Date:

1972-11-01

Pagination or Media Count:

18.0

Abstract:

Synthesis of several aliphatic and aromatic amides and diamides are described in this report. The compounds infrared spectra are given. These are candidate compounds as high-temperature liquid phases to be used in gas chromatography for the class separation of aromatic and aliphatic hydrocarbon compounds. The compounds discussed are N,N-bis2-cyanoethylbenzoyl amide, 4- methoxy-N,N-biscyanoethylbenzoyl amide, 4-cyano-N,N-bis2-cyanoethylbenzoyl amide, N,N-tetra2-cyanoethyloxalya diamide, and N,N-tetra2cyanoethyladipyl diamide.

Descriptors:

• *AMIDES
• *NITRILES
• SYNTHESIS(CHEMISTRY)
• INFRARED SPECTRA
• GAS CHROMATOGRAPHY

Subject Categories:

• Organic Chemistry

Distribution Statement:

APPROVED FOR PUBLIC RELEASE