Accession Number:

AD0742484

Title:

Rubber Research: The Synthesis of Unsaturated Fluorocarbons

Descriptive Note:

Technical Report,13 Aug 1960,13 Nov 1960

Corporate Author:

COLORADO UNIV AT BOULDER BOULDER

Personal Author(s):

Report Date:

1960-12-10

Pagination or Media Count:

12.0

Abstract:

The report describes the synthesis of CF2Cl-CF2NO using NOCl and FeCl3 as a catalyst. The FeCl3 also forms an addition complex with the nitorso compound. The compound, UO2NO32H2ON2O4, was used to nitrate CF2CFCl as a means of producing nitroso compounds by stopping the reaction before completion. The reduction of fluoronitro alkanes was also tried. As a precursor to imine synthesis, CF3-CF2-CF2-CHOH-CH2NO2 was prepared.

Subject Categories:

  • Organic Chemistry

Distribution Statement:

APPROVED FOR PUBLIC RELEASE