Rubber Research: The Synthesis of Unsaturated Fluorocarbons
Technical Report,13 Aug 1960,13 Nov 1960
COLORADO UNIV AT BOULDER BOULDER
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The report describes the synthesis of CF2Cl-CF2NO using NOCl and FeCl3 as a catalyst. The FeCl3 also forms an addition complex with the nitorso compound. The compound, UO2NO32H2ON2O4, was used to nitrate CF2CFCl as a means of producing nitroso compounds by stopping the reaction before completion. The reduction of fluoronitro alkanes was also tried. As a precursor to imine synthesis, CF3-CF2-CF2-CHOH-CH2NO2 was prepared.
- Organic Chemistry