A Lattice Parameter Method for Determining the Composition of NH4Cl04/KCl04 Solid Solution.
PICATINNY ARSENAL DOVER N J
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The lattice parameters of eight samples of NH4ClO4, KClO4, and NH4ClO4KClO4 solid solutions were determined by photographic powder x-ray diffraction. With the aid of a computer, the parameters were calculated utilizing both least squares analysis and successive approximations techniques. The data indicated that, at the present time, the method could be used for analysis of NH4ClO4KClO4 solid solutions containing less than 20 mole percent KClO4. Author