Accession Number:

AD0711194

Title:

THE CRYSTAL STRUCTURE OF N-METHYLRHOEAGENINE IODIDE,

Descriptive Note:

Corporate Author:

NATIONAL RESEARCH COUNCIL OF CANADA OTTAWA (ONTARIO) BIOCHEMISTRY LAB

Personal Author(s):

Report Date:

1969-05-12

Pagination or Media Count:

10.0

Abstract:

The structure and stereochemistry of N-methylrhoeagenine iodide have been determined by three-dimensional Fourier and least-squares methods using visually estimated intensity data. The crystals have orthorhombic symmetry, space group C2221, with a 8.54, b 26.19 A,Z 8. The two 1,3-benzodioxole systems, which are linked by cis-fused azacycloheptene and dihydropyran rings, are nearly mutually perpendicular. The hydroxyl group and the hydrogen atoms at the junction of the two heterocyclic rings lie on the same side of the dihydropyran ring. Infinite chains of alternating iodide ions and organic cations are arranged parallel to the 110 direction. Author

Subject Categories:

  • Organic Chemistry
  • Crystallography

Distribution Statement:

APPROVED FOR PUBLIC RELEASE