AN IMPROVED SYNTHESIS OF 1,6-DICARBACLOSODECABORANE(10).
CALIFORNIA UNIV LOS ANGELES DEPT OF CHEMISTRY
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Hydroboration of a diethyl ether solution of NaB7C2H13B7C2H13 yields 1,6-B8C2H10 in 74 yield. Recovery of the unreacted B7C2H13 raises the yield to 82. The C-monomethyl, C,C-dimethyl, and C-monophenyl derivatives of 1,6-B8C2H10 can be prepared in somewhat higher yields. Author
- Inorganic Chemistry
- Organic Chemistry