PERCHLORATE ESTER: PREPARATION AND POLYMERIZATION
Technical rept. 1 Jan 1960-1 Jan 1961
AERONAUTICAL SYSTEMS DIV WRIGHT FIELD OH
Pagination or Media Count:
Epiperchloratohydrin I was synthesized and polymerized although covalent perchlorates are known to be hydrolytically unstable. Compound I, dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound I before and after polymerization was explosive and required special care.
- Organic Chemistry