Accession Number:

AD0691014

Title:

PERCHLORATE ESTER: PREPARATION AND POLYMERIZATION

Descriptive Note:

Technical rept. 1 Jan 1960-1 Jan 1961

Corporate Author:

AERONAUTICAL SYSTEMS DIV WRIGHT FIELD OH

Personal Author(s):

Report Date:

1961-09-01

Pagination or Media Count:

9.0

Abstract:

Epiperchloratohydrin I was synthesized and polymerized although covalent perchlorates are known to be hydrolytically unstable. Compound I, dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound I before and after polymerization was explosive and required special care.

Subject Categories:

  • Organic Chemistry

Distribution Statement:

APPROVED FOR PUBLIC RELEASE