SYNTHESIS AND POLYMERIZATION OF FLUORINATED SULFUR MODIFIED NITROSO RUBBER
Technical Report,01 Jul 1965,26 Nov 1965
PENINSULAR CHEMRESEARCH GAINESVILLE FL GAINESVILLE
Pagination or Media Count:
Terpolymer samples containing 3 and 6 mole percent ONCF2CF2CO2CH3 with CF3NO and CF2CF2 were prepared. A larger amount 280 g. of 1,1,2-trifluorobutadiene terpolymer with CF3NO and CF2CF2 was prepared. Terpolymers of CF2CFCF2NO, CF2CFCH2CF2CF2CH2CFCF2 and ONCF2CF2CF2COOH with CF3NO and CF2CF2 were prepared. Attempted copolymerization of carbonyl fluoride and hexafluoroacetone with CF3NO was unsuccessful. A 2-1. reactor equipped with stirrer and cooling coils has been procured and is being fitted with a refrigeration system.