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HIGH ENERGY OXIDIZERS
Quarterly technical summary rept. for 1 May-31 Jul 1965
STAUFFER CHEMICAL CO RICHMOND CA WESTERN RESEARCH CENTER
Pagination or Media Count:
Infrared and conductivity measurements show that MClF4 where M is NO, Rb, or Cs is ionic in the solid state and in solution, respectively. A square-planar structure point group D4h is assigned to the ClF4- anion in Rb ClF4- and Cs ClF4-. For the ClF4- anion in NO ClF4- the low-temperature infrared measurement indicates a lower symmetry at least as low as point group D2h. A vacuum line, which will enable running glow-discharge reactions at low temperatures and reduced pressures, was designed and built. Density measurements on the alkali metal difluorochlorates I indicate that the X-ray patterns given in the preceding Quarterly Report are probably due to small amounts of alkali metal bifluorides, present as impurities.
APPROVED FOR PUBLIC RELEASE