Accession Number:

AD0618158

Title:

CRYSTAL STRUCTURE OF HETERATISINE HYDROBROMIDE MONOHYDRATE,

Descriptive Note:

Corporate Author:

NATIONAL RESEARCH COUNCIL OF CANADA OTTAWA (ONTARIO) DIV OF PURE CHEMISTRY

Personal Author(s):

Report Date:

1964-07-23

Pagination or Media Count:

5.0

Abstract:

The space group of heteratisine hydrobromide monohydrate, C22H33O5N.HBr.H2O is P2 sub 1 and the unit-cell dimensions are a 8.96, b 14.54, c 8.55 A, beta 90 degrees 40, Z 2. The structure was solved from a three-dimensional Fourier synthesis by the heavy-atom method. No chemical assumptions were made, except that the nitrogen atom was identified by comparison of the skeleton with that of lycoctonine. Refinement was carried out by the least-squares method. Author

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Distribution Statement:

APPROVED FOR PUBLIC RELEASE