X-RAY CRYSTALLOGRAPHIC STUDIES OF AMINOBORANES AND RELATED COMPOUNDS.
Final technical rept. no. 1, 1 Oct 62-31 Mar 64,
BIRKBECK COLL LONDON (ENGLAND)
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The lattice parameters and space groups of crystals of five compounds containing B-N bonds were determined, by means of X-ray photographs, as a preliminary to a detailed X-ray structure analysis of some of these substances. Compounds studied were B-trifluoroborazole diisopropylamino diphenylborane diisopropylamino di-p-bromophenyl borane bi-1,3-demethyl-1,3,2-diazaborolidin-2-yl and 1,4-diphenyl2,3,5,6-tetramethyl-2,3,5,6-tetraza-1,4-diborine. Diisopropylamino-p-bromophenyl-phenylborane was also examined but it proved impossible to produce single crystals of this compound suitable for X-ray work.