SYNTHESIS OF STEROESPECIFIC AMINOTHIOLS AS RADIOPROTECTIVE AGENTS.
Progress rept., 1 Jul 62-1 Mar 63,
CALIFORNIA UNIV SAN FRANCISCO MEDICAL CENTER
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The synthesis of cis-2-aminocyclopentanthiol from 2methylcyclopentanothiazoline was found to be not practicable. The following were obtained as intermediates S,N,Ntribenzol-cis-2-aminocyclopentane m.p. 167-1680 S-acetyl-cis-2-benzamidocyclopentane thiol m.p. 132-133C S-acetyl-cis-2-acetamidocyclopentane thiol m.p. 63-64C cis-1-acetyl-2-methyl-4-oxobicyclo-5.0.3-1-aza-5thiadec-2-ene m.p. 137.5-139C.