Accession Number:

AD0466120

Title:

NITROSO RUBBER RESEARCH, DEVELOPMENT AND PRODUCTION

Descriptive Note:

Technical Report,27 Feb 1963,31 May 1963

Corporate Author:

THIOKOL CORP TRENTON NJ TRENTON United States

Personal Author(s):

Report Date:

1963-05-31

Pagination or Media Count:

29.0

Abstract:

The preparation of trifluoroacetyl nitrite by the interaction of trifluoroacetic anhydride and dinitrogen trioxide has been effected by replicate, small scale batches. Exploratory solution pyrolyses of the nitrite indicate that decarboxylation occurs at temperatures of 145 C or greater. Trifluoronitrosomethane was the major product. Small quantities of nitrosyl fluoride FNO, for the synthesis of improved low temperature nitroso rubbers, were prepared by pyrolysis of nitrosyl tetrafluoroborate NOBF4 and sodium fluoride at 250 C.

Subject Categories:

Distribution Statement:

APPROVED FOR PUBLIC RELEASE