Accession Number:

AD0292908

Title:

THE SYNTHESIS OF AMINO-1,2-DITHIACYCLANES

Descriptive Note:

Corporate Author:

RENSSELAER POLYTECHNIC INST TROY N Y

Personal Author(s):

Report Date:

1962-08-01

Pagination or Media Count:

1.0

Abstract:

Cyclic amino disulfides with varying degrees of ring - strain and related dimercaptoamines were prepared. Rearrangement of nitrogen mustardlike intermediates was prevented by blocking the nitrogen with the benzenesulfonyl group prior to the introduction of the sulfur - containing functions. If the nitrogen was not in a position propitious for ring closure and rearrangement, blocking of the nitrogen was unnecessary. Nor were rearrangements of concern when the amino group was introduced subsequent to the introduction of the sulfur functions. Author

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Distribution Statement:

APPROVED FOR PUBLIC RELEASE