SYSTEMS CONTAINING A SILICON-OXYGEN-METAL LINKAGE
INORGANIC RESEARCH LAB WESTERN RESERVE UNIV CLEVELAND OHIO
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Methods were developed for the preparation of the vanadium siloxy esters tristriphenylsiloxy vanadate and tristriphenylsiloxy thiovanadate. Modifications of the reported methods to give high yields of tetrakistriphenylsiloxy vanadium are discussed. A quick and accurte method for the quantitative determination of Si and V in these esters was developed.