Accession Number : AD0439242


Title :   SYNTHESIS OF SELECTED ETHERS, PHENOLS AND RELATED COMPOUNDS HAVING NITROGEN-CONTAINING GROUPS.


Descriptive Note : Final rept., 1 Oct 61-31 Mar 64,


Corporate Author : BOSTON UNIV MASS


Personal Author(s) : Mason,J Philip ; mcInnis,Raymond G ; Hennessy,Harry L ; Lord,Pierre D ; Eaton,John E


Report Date : 31 Mar 1964


Pagination or Media Count : 53


Abstract : The work done under Contract No. DA-18-108-CML6678 and the extension of this contract can best be reported in three categories. The first, Part A, is a continuation of work done on prior grants and contracts to complete the series of compounds which can be described as alpha-3nitrophenoxy-omega-(3-nitro-5-dimenthylcarbamyloxyphenoxy)-alkanes and alpha-(3-nitrophenoxy)omega-(3-nitro-5-hydroxyphenoxy)-alkanes. Some 1,10-bis(3-nitro-5-dimethylcarbamyloxyphenoxy)decane was also prepared. Part B of this report contains the methods used for the preparation of various intermediates to be used in the synthesis of 1,3-bid(5-dimethylcarbamyloxy-3pyridoxy)-propane and 1-(3-pyridoxy)-3-(5dimethylcarbamyloxy-3-pyridoxy)-propane. Part C contains the methods of preparing various aliphatic compounds containing two tertiary amine groups and two alcohol groups, or groups which could be converted to alcohols. Much of this work was left in an incomplete state when it was decided to abandon work with the aliphatic compounds. (Author)


Descriptors :   *ORGANIC NITROGEN COMPOUNDS , *PHENOLS , *ETHERS , SYNTHESIS(CHEMISTRY) , SYNTHESIS(CHEMISTRY) , SYNTHESIS(CHEMISTRY) , NITRATES , ALCOHOLS , ALKANES , NITROGEN HETEROCYCLIC COMPOUNDS , AMINES , PYRIDINES , CARBAMIC ACID , HYDROXIDES , AROMATIC COMPOUNDS , ORGANIC SULFUR COMPOUNDS , BROMINE COMPOUNDS , CHLORINE COMPOUNDS , HYDROLYSIS , MOLECULAR STRUCTURE


Distribution Statement : APPROVED FOR PUBLIC RELEASE